IP 391: Petroleum products - Determination of aromatic hydrocarbon types in middle distillates - High performance liquid chromatography method with refractive index detection

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  • Method adopted/last revised: 2007
  • Method reapproved: None
  • REF/ISBN: IP391-2934869
  • Status: Current
  • First printed in STM books: January 2007

Scope

This European Standard specifies a test method for the determination of the content of mono-aromatic,di-aromatic and tri+-aromatic hydrocarbons in diesel fuels that may contain fatty acid methyl esters (FAME) up to 5 % (V/V) and petroleum distillates in the boiling range from 150 °C to 400 °C. The polycyclic aromatic hydrocarbons content is calculated from the sum of di-aromatic and tri+-aromatic hydrocarbons and the total content of aromatic compounds is calculated from the sum of the individual aromatic hydrocarbon types. Compounds containing sulfur, nitrogen and oxygen may interfere in the determination; mono-alkenes do not interfere, but conjugated di-alkenes and polyalkenes, if present, may do so.

The precision statement of the test method has been established for diesel fuels with and without FAME blending components, with a mono-aromatic content in the range from 6 % (m/m) to 30 % (m/m), a di-aromatic content from 1 % (m/m) to 10 % (m/m), a tri+-aromatic content from 0 % (m/m) to 2 % (m/m), a polycyclic aromatic content from 1 % (m/m) to 12 % (m/m), and a total aromatic content from 7 % (m/m) to 42 % (m/m).

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